- RIUMA Principal
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- Química Inorgánica, Cristalografía y Mineralografía - (QICM)
- QICM - Artículos
- Listar QICM - Artículos por autor
Listar QICM - Artículos por autor "León-Reina, Laura"
Mostrando ítems 1-18 de 18
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A Self-Folding Polymer Film Based on Swelling Metal–Organic Frameworks
Troyano, Javier; Carné-Sánchez, Arnau; Pérez-Carvajal, Javier; León-Reina, Laura; Imaz, Inhar; Cabeza-Díaz, Aurelio; Maspoch, Daniel[et al.] (Wiley-VCH Verlag GmbH & Co., 2018-10-23)Herein, we exploit the well-known swelling behaviour of metal–organic frameworks (MOFs) to create a selffolding polymer film. Namely, we show that incorporating crystals of the flexible MOF MIL-88A into a polyvinylidene ... -
Accuracy in Cement Hydration Investigations: Combined X-ray Microtomography and Powder Diffraction Analyses
Salcedo, Inés R.; Cuesta-García, Ana María; Shirani, Shiva; León-Reina, Laura; García-Aranda, Miguel Ángel (MDPI, 2021-11-17)Cement hydration is a very complex set of processes. The evolution of the crystalline phases during hydration can be accurately followed by X-ray powder diffraction data evaluated by the Rietveld method. However, accurate ... -
Accuracy in Rietveld quantitative phase analysis: a comparative study of strictly monochromatic Mo and Cu radiations
León-Reina, Laura; García-Maté, Marta; Álvarez-Pinazo, Gema; Santacruz-Cruz, María Isabel; Vallcorba, Oriol; Gómez-de-la-Torre, María de los Ángeles; García-Aranda, Miguel Ángel[et al.] (Willey online Library, 2016)This study reports 78 Rietveld quantitative phase analyses using Cu K 1, Mo K 1 and synchrotron radiations. Synchrotron powder diffraction has been used to validate the most challenging analyses. From the results for ... -
Amorphous determination in calcium sulfoaluminate materials by external and internal methods
García-Maté, Marta; Santacruz-Cruz, María Isabel; Cuesta-García, Ana María; León-Reina, Laura; García-Aranda, Miguel Ángel; Baco, Isabelle; Morin, Vincent; Walenta, Günther; Gartner, Ellis; Gómez-de-la-Torre, María de los Ángeles[et al.] (ICE Publishing, 2014)External standard methodology has been successfully applied to quantify the known amounts of amorphous component that are increasingly added to cement-related materials. The consistency and accuracy of the methodology were ... -
Effect of calcium sulfate source on the hydration of calcium sulfoaluminate eco-cement
García-Maté, Marta; Gómez-de-la-Torre, María de los Ángeles; León-Reina, Laura; Ramírez-Losilla, Enrique; García-Aranda, Miguel Ángel; Santacruz-Cruz, María Isabel[et al.] (2014)The availability of cements, including eco-cements, with tailored mechanical properties is very important for special applications in the building industry. Here we report a full study of the hydration of calcium sulfoaluminate ... -
Guest Molecule-Responsive Functional Calcium Phosphonate Frameworks for Tuned Proton Conductivity
Bazaga-García, Montse; Pérez-Colodrero, Rosario Mercedes; Papadaki, M.; Garczarek, Piotr; Zon, Jerzy; Olivera-Pastor, Pascual; Losilla, Enrique R.; León-Reina, Laura; García-Aranda, Miguel Ángel; Choquesillo-Lazarte, Duane; Demadis, Konstantinos D.; Cabeza-Díaz, Aurelio[et al.] (American Chemical Society, 2014-03-18)We report the synthesis, structural characterization, and functionality of an open-framework hybrid that combines Ca2+ ions and the rigid polyfunctional ligand 5-(dihydroxyphosphoryl) isophthalic acid (PiPhtA). Ca-PiPhtA-I ... -
High Proton Conductivity in a Flexible, Cross-Linked, Ultramicroporous Magnesium Tetraphosphonate Hybrid Framework
Pérez-Colodrero, Rosario Mercedes; Olivera-Pastor, Pascual; Losilla, Enrique R.; Hernández Alonso, Daniel; García-Aranda, Miguel Ángel; León-Reina, Laura; Rius, Jordi; Demadis, Konstantinos D.; Moreau, Bernard; Villemin, Didier; Palomino, Miguel; Rey, Fernando; Cabeza-Díaz, Aurelio[et al.] (American Chemical Society, 2012-07-03)Multifunctional materials, especially those combining two or more properties of interest, are attracting immense attention due to their potential applications. MOFs, metal organic frameworks, can be regarded as multifunctional ... -
Hydration Reactions and Mechanical Strength Developments of Iron- Rich Sulfobelite Eco-cements
Álvarez-Pinazo, Gema; Santacruz-Cruz, María Isabel; León-Reina, Laura; García-Aranda, Miguel Ángel; Gómez-de-la-Torre, María de los Ángeles (2013)Belite calcium sulfoaluminate (BCSA) cements are low-CO2 building materials. However, their hydration behavior and its effect on mechanical properties have still to be clarified. Here, we report a full multitechnique study ... -
Hydration studies of calcium sulfoaluminate cements blended with fly ash
García-Maté, Marta; Gómez-de-la-Torre, María de los Ángeles; León-Reina, Laura; García-Aranda, Miguel Ángel; Santacruz-Cruz, María Isabel (Elsevier, 2013)The main objective of this work is to study the hydration and properties of calciumsulfoaluminate cement pastes blended with fly ash (FA) and the corresponding mortars at different hydration ages. Laboratory X-ray ... -
Mix and measure - Combining in situ X-ray powder diffraction and microtomography for accurate hydrating cement studies.
Shirani, Shiva; Cuesta-García, Ana María; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; Koufany, Imane; Redondo-Soto, Cinthya; Ruiz Salcedo, Inés; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (Elsevier, 2023-11-14)It is reported an innovative methodology based on in situ MoKα1 laboratory X-ray powder diffraction (LXRPD) and microtomography (μCT) avoiding any sample conditioning. The pastes are injected in 2.0 mm capillaries and the ... -
Multifunctional lanthanum tetraphosphonates: Flexible, ultramicroporous and proton-conducting hybrid frameworks
Pérez-Colodrero, Rosario Mercedes; Olivera-Pastor, Pascual; Losilla, Enrique R.; García-Aranda, Miguel Ángel; León-Reina, Laura; Papadaki, M.; McKinlay, Alistair C.; Morris, Russell E.; Demadis, Konstantinos D.; Cabeza-Díaz, Aurelio[et al.] (The Royal Society of Chemistry, 2012)A new flexible ultramicroporous solid, La(H5DTMP)·7H2O (1), has been crystallized at room temperature using the tetraphosphonic acid H8DTMP, hexamethylenediamine-N,N,N′,N′-tetrakis(methylenephosphonic acid). Its crystal ... -
Multifunctional Luminescent and Proton-Conducting Lanthanide Carboxyphosphonate Open-Framework Hybrids Exhibiting Crystalline-to-Amorphous-to-Crystalline Transformations
Pérez-Colodrero, Rosario Mercedes; Papathanasiou, Konstantinos E.; Stavgianoudaki, Nikoleta; Olivera-Pastor, Pascual; Losilla, Enrique R.; García-Aranda, Miguel Ángel; León-Reina, Laura; Sanz, Jesús; Sobrados, Isabel; Choquesillo-Lazarte, Duane; García-Ruíz, Juan M.; Atienzar, Pedro; Rey, Fernando; Demadis, Konstantinos D.; Cabeza-Díaz, Aurelio[et al.] (American Chemical Society, 2012-09-15)The chemistry of metal phosphonates has been progressing fast with the addition of new materials that possess novel structural features and new properties, occasionally in a cooperative manner. In this paper, we report a ... -
Rheological and hydration characterization of calcium sulfoaluminate cement pastes
García-Maté, Marta; Santacruz-Cruz, María Isabel; Gómez-de-la-Torre, María de los Ángeles; León-Reina, Laura; García-Aranda, Miguel Ángel (2015-05-14)Calcium sulfoaluminate (CSA) cements are currently receiving a lot of attention because their manufacture produces less CO2 than ordinary Portland cement (OPC). However, it is essential to understand all parameters which ... -
Rietveld quantitative phase analyses of SRM 2686a: a standard Portland clinker
García-Maté, Marta; Álvarez-Pinazo, Gema; León-Reina, Laura; Gómez-de-la-Torre, María de los Ángeles (2018-10-03)SRM 2686a is a NIST reference Portland clinker with reported mineralogical analysis from powder diffraction and electron microscopy. This sample is used in ASTM C1365 test method for Rietveld quantitative phase analysis ... -
Rietveld Quantitative Phase Analysis of OPC Clinkers, Cements and Hydration Products
García-Aranda, Miguel Ángel; Gómez-de-la-Torre, María de los Ángeles; León-Reina, Laura (Mineralogical Society of America, 2012) -
Rietveld quantitative phase analysis of yeelimite-containing cements
Álvarez-Pinazo, Gema; Cuesta-García, Ana María; García-Maté, Marta; Santacruz-Cruz, María Isabel; Ramírez-Losilla, Enrique; Gómez-de-la-Torre, María de los Ángeles; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (Karen Scrivener, 2012)Yeelimite-containing cements are attracting attention for their tailored properties. Calcium sulfoaluminate, CSA, cements have high contents of Yeelimite and they are used for special applications. Belite calcium sulfoaluminate, ... -
Rietveld quantitative phase analysis of Yeelimite-containing cements
Álvarez-Pinazo, Gema; Cuesta-García, Ana María; García-Maté, Marta; Santacruz-Cruz, María Isabel; Ramírez-Losilla, Enrique; Gómez-de-la-Torre, María de los Ángeles; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (Elsevier, 2012-03-26)Yeelimite-containing cements are attracting attention for their tailored properties. Calcium sulfoaluminate, CSA, cements have high contents of Yeelimite and they are used for special applications. Belite calcium sulfoaluminate, ... -
Rietveld quantitative phase analysis with molybdenum radiation
Cuesta-García, Ana María; Álvarez-Pinazo, Gema; García-Maté, Marta; Santacruz-Cruz, María Isabel; García-Aranda, Miguel Ángel; Gómez-de-la-Torre, María de los Ángeles; León-Reina, Laura[et al.] (Cambridge Core, 2014)Building materials are very complex samples of worldwide importance; hence quantitative knowledge of their mineralogical composition is necessary to predict performances. Rietveld quantitative phase analysis (RQPA) allows ...